nipponalba | pleroma

After 17 days in the fermenter (much longer than I normally leave it), Iโ€™ve transferred my latest imperial stout into a keg.

In order to try and nail whether my โ€˜too much yeast in sampleโ€™ theory on preciously misses final gravity targets was correct, I took samples at start, ~25%, ~50% and ~75% of the way through the transfer for refractometer measures and an additional hydrometer sample at ~75%.

Somewhat frustratingly the refractometer result was the same for all 4 samples and around the same high level of previous brews (around 1.042 specific gravity)..

.. however the hydrometer returnes 1.022 a mere 0.006 above my final target!

One of these devices requires tuning (by a clueless me) and the other is likely accurate!

So the estimated ABV on the brewsheet is 8.9% (though the brewerโ€™s friend calculator corrects that to 8.8%) and I have hit 8.01%!

I shall celebrate in a few weeks once it has carbonated!


(https://jk.nipponalba.scot/photo/5f7e1d5c/)
shot of hydrometer resting at 1.02SG in a beaker of imperial stout

This was just the lift I needed after a tough few days of trying to get my head around microbial metabolism!

@athairbirb it's a sealed glass apparatus with ball bearings, wax(?) and floats to measure the density of sugar, the more sugar the higher it floats.

The refractometer requires manual tuning and it could be that I've not done that well, maybe the water when doing so was way too cold or something. So of the two, much less likely to be accurate.

It makes sense as my beer a few brews ago kicked like a mule, but according to my measurements merely breaches 4%.. I suspect that if I'd used the hydrometer it would have told a different story!
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Errr preciously misses = previously missed

@jk @athairbirb
I've used various refractometers over the years. They are very sensitive to temperature.
Ive seen me have to adjust the calibration a few times over the course of a day. The last instrument I used was quite old though.
What do you use to calculate yours?

@wizardofosmium
I calibrated it with water, but I suspect it was too cold. So I am pleased to see you mention temperature sensitivity!

Calculations? Just reading the specific gravity, then entering the Original and Final gravity figures into the Brewer's Friend website calculator. Still very much a novice in this respect.

I tuned it to the same measurement as the hydrometer with the correct temperature wort so will see if it is even close to the original gravity next time I brew!

@athairbirb

@jk @athairbirb
When I last used one we had to check the calibration with purified water and a certified test piece at 20ยบC +/- 0.5ยบC before we could use it for analysis. The instrument had a built in temperature probe and had cooled/heated water pumped through it to maintain the temp.
Others I've used in the past didn't have the water to maintain the temp but we made sure that the sample was at the correct temp.
Occasionally some samples tested were done at 16ยบC.

@jk @athairbirb
This is a link to an older edition of the European pharmacopoeia extract detailing the requirements
http://library.njucm.edu.cn/yaodian/ep/EP5.0/02_methods_of_analysis/2.2.__physical_and_physicochemical_methods/2.2.7.%20Optical%20rotation.pdf

There's a bit about viscosity on the next page you may find interesting.
I've used all the techniques mentioned on those pages.

@wizardofosmium Interesting, this one isn't anywhere nearly as advanced as that, just has a screw to adjust to calibrate.

@athairbirb
Simple refractometer, with rubber black handle, silver body and blue glass plate.

@wizardofosmium Thank you! I've saved the PDF and shall peruse later!
@athairbirb

@athairbirb @wizardofosmium I guess that could be one of the problems then, I just used tap water.